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Analytical Chemistry of Molybdenum

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Table of Contents

1 Introduction.- 2 Detection.- 1. Detection in the Presence of Many Ions.- 2. Spot Tests.- 3. Detection in Specific Materials.- 3 Separations.- 1. Precipitation.- 2. Extraction.- 3. Ion Exchange.- 4. Paper and Thin Layer Chromatography.- 5. Other Separation Techniques.- 6. Applications of Specific Materials.- 4 Gravimetric Methods.- 1. Precipitation with Sulfide Ion.- 2. Precipitation as Molybdate Ion.- 2.1 Lead Molybdate.- 2.2 Other Molybdates.- 3. Precipitation with Organic Reagents.- 3.1 8-Hydroxyquinoline.- 3.2 ?-Benzoinoxime.- 3.3 Other Organic Precipitating Agents.- 4. Applications to Specific Materials.- 5 Titrimetric Methods.- 1. Precipitation Titrations.- 1.1 With Various Metals.- 1.2 With Organic Reagents.- 2. Complexometric Titrations.- 3. Oxidation-Reduction Titrations.- 3.1 Reactions with Oxidizing Agents.- 3.2 Reactions with Reducing Agents.- 4. Applications to Specific Materials.- 6 Colorimetric Methods.- 1. Color Forming Reagents.- 1.1 Thiocyanate Ion.- 1.2 Toluene-3,4-dithiol.- 1.3 Other Color Forming Agents.- 2. Applications to Specific Materials.- 7 Emission Spectroscopy.- 1. General Considerations.- 2. Laboratory Procedures.- 3. Applications to Specific Materials.- 8 Atomic Absorption Spectrometry.- 1. General Considerations.- 2. Laboratory Procedures.- 3. Applications to Specific Materials.- 9 X-Ray Fluorescence.- 1. General Considerations.- 2. Laboratory Procedures.- 3. Applications to Specific Materials.- 10 Voltammetry.- 1. Polarography.- 2. Anodic Stripping Voltammetry.- 3. Applications to Specific Materials.- 11 Catalytic Methods.- 1. Hydrogen Peroxide - Iodide Reaction.- 2. Other Molybdenum Catalyzed Reactions.- 3. Applications to Specific Materials.- 12 Radiochemical and Activation Methods.- 1. Radioactive Molybdenum Isotopes.- 1.1 Determining Radioactive Molybdenum.- 1.2 Isotopic Dilution with Radioactive Molybdenum.- 2. Activation Analysis.- 3. Applications to Specific Materials.- 13 Rocks and Mineral Samples.- 14 Molybdenum and Molybdenum Based Alloys.- 15 Molybdenum in Ferrous Alloys.- 16 Molybdenum in Non-Ferrous Alloys.- 17 Molybdenum Compounds.- 18 Animal, Plant, and Soil Samples.- 1. Animal Samples.- 2. Plant Samples.- 3. Soil Samples.- 19 Environmental Samples.- 1. Water Samples.- 2. Air Samples.- 3. Fuels Samples.- 20 Miscellaneous Samples.- Author Index.

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