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Methods for the Analysis of Iron and Steel Used in Laboratories of the American Rolling Mill Co;, Middletown, Ohio
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Excerpt from Methods for the Analysis of Iron and Steel Used in Laboratories of the American Rolling Mill Co;, Middletown, Ohio Dissolve grams of the sample in a plati num dish, using 60 c. C. Of nitric acid, specific gravity, and 10 c. C. Of sulphuric acid, specific gravity. Evaporate to dense white fumes and allow to cool. Dissolve ferric sul phate in about 35 c. C. Of hydrochloric acid, specific gravity, dilute and filter. Filter on ashless paper and wash alternately with distilled water and dilute hydrochloric acid, specific gravity, until free from iron. Ignite in platinum crucible, using a lvieker burner with natural draft. Weigh residue and add about 1 c. C. Of hydro uoric acid and about 3 drops of coneen trated sulphuric acid. Heat crucible carefully until acid has evaporated, then to full temper ature of burner until iron has changed to oxide. Cool and weigh. The loss is silica. Each milligram equals 01% of silicon. About the Publisher Forgotten Books publishes hundreds of thousands of rare and classic books. Find more at www.forgottenbooks.com This book is a reproduction of an important historical work. Forgotten Books uses state-of-the-art technology to digitally reconstruct the work, preserving the original format whilst repairing imperfections present in the aged copy. In rare cases, an imperfection in the original, such as a blemish or missing page, may be replicated in our edition. We do, however, repair the vast majority of imperfections successfully; any imperfections that remain are intentionally left to preserve the state of such historical works."
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